Top loading 3He refrigerator, HelioxTMTL

HelioxTL Top loading 3He sorption pump refrigerator

A sample-in-liquid 3He refrigerator that provides a simple means of cooling samples below 260 mK for over 50 hours.

  • Top loading into the mixture ensures good thermalisation and high stability of the thermal environment
  • Quick and easy sample change : the sample fitted on the top loading probe can be removed quickly while the insert remains cold. A vacuum lock mechanism ensures there is no loss of 3He or entry of air into the sample space.
  • Multi-service access - provides a unique platform that can be used with a range of sample probes such as Swedish rotators and high frequency coaxial lines.

This design of this system is unique and protected by patent US5829270.

  • Specifications 
  • System components/options 
  • Operation 
  • Applications 
  • Images 

Temperature range

<260 mK – 1.2 K Higher temperature option available on request. (up to 80 K)

Cooling power

>400 µW at 300 mK for over 6 hrs

Temperature stability

±3 mK below 1.2K (on the probe)

Operating time at base temperature (no heat load)

>50 hrs

3He regeneration time

Typically 50 min

Liquid helium consumption (typical) 2 litres to cool the probe to 4K. 0.05 l/hr additional consumption to run

Sample space access

38 mm diameter

Minimum room height requirements

3.7 m  with SMD10/15VS cryostat and 4.1 m with SMD 10/15VSEX cryostat.

A HelioxTL system consists of :

  • An insert - including the sorb, the 1 K pot and the 3He pot
  • A probe or combination of probes (experimental access and wiring)
  • External 3He dump

Options:

  •   A range of non-standard top-loading probes
  •  Pumping manifold for 1 K pot (rotary pump, pumping lines, vacuum valves and gauge)
  •  Calibrated ruthenium oxide sensors on the 3He pot
  •  80K high temperature option

Solution to helium rising costs:

The Heliox TL is compatible the IntegraAC, recondensing liquid helium cryostat.

This product has been developed to significantly reduce the consumption of liquid helium by recondensing helium gas evaporated within the system, which would other wise be vented from the cryostat. This decreases the frequency of helium refills. Cryogenic systems can be kept cold continuously, even when in stand by mode, leading to greater freedom to schedule experimental time.

IntegraAC recondensing dewar compability sketch

The sample is mounted onto the top-loading probe and inserted directly into the 3He liquid through the central access of the insert. A vacuum lock allows the sample to be inserted and withdrawn without loss of 3He or entry of air into the sample space.

When the probe has been inserted, the sorb is warmed to over 30 K. This recondenses the 3He gas on the 1K pot assembly which runs down to cool the sample. At this stage the sample is surrounded by 3He liquid at approximately 1.2 K. The sorb is then cooled, and it begins to reduce the vapour pressure above the liquid 3He to decrease the sample temperature. The minum temperature possible in this type of refrigerator is approximately 250 mK with no experimental heat load.

HelioxTL top loading insert mode of operation

Research areas

Applications

Experimental techniques
Semiconductors Quantum Hall Effect
Quantum dots
Single electron tunneling
Quantum computing
Magneto-resistance
Hall effect
RF transport
High frequency conductivity
Solid State Physics Heavy fermions systems
Metal insulator transition
Spin glass
Mesoscopic systems
Giant magnetic resistance
Specific heat
DeHaas-van Alphen Oscillations
Solid state NMR
Electrical resistivity
Magneto-resistance
Neutron scattering
Superconductivity Low Tc superconductors
Quantum computing  
Josephson junctions
Flux vortices
Quantum initial phenomema
Electrical resistivity
Scanning spectroscopy(STM/AFM)
Squids
AC susceptibility
Astrophysics & Cosmology Low temperature detectors Superconducting tunnel junctions
Ge bolometers
Electrothermal measurements
Voltage biased measurements
Low energy photon detection
Metrology Quantum Hall Effect
Voltage standards
Current standards
Magneto-resistance
DC & AC low frequency transport and magnetic measurements
Single electron tunneling

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